Your questions answered

Find answers to common questions about the Thermo Scientific iQ Series instruments. Draw on our expertise to fully utilize your instruments’ potential.


FAQs for gas analyzers

Communications

In addition to the wireless and ethernet communications protocols, digital and analog I/O communications are still supported. All supported methods to connect to the instrument can be found in the iQ Series Communication manual.

Currently wireless connectivity to the iQ series platform is capable via a wireless ethernet bridge. A wireless ethernet bridge is a commercial off-the-shelf intelligent network device that can be utilized to provide wireless ethernet capabilities to Thermo Fisher Scientific’s instruments that have only a wired ethernet port. A single bridge may be used to provide wireless ethernet to one or more instruments and may be mounted indoors or outdoors at a location up to 300 feet away from the instrument to provide optimal wireless coverage.

A VPN server would have to exist within the network that the instrument is expected to operate. Local IT would need to ensure a VPN server is set up and available to facilitate the connection of multiple instruments. All supported methods to connect to the instrument can be found in the iQ Series Communication manual.

A total of 11 email addresses can be saved in the instrument: 1 primary contact and 10 courtesy copy (CC) contacts. You cannot discriminate what content goes to which email contacts. All emails generated by the instrument will be sent to the primary contact as well as any CC contacts listed.

The iQ Series analyzers are both dynamic and static IP address capable. Choosing the desired operating configuration can be set in the ‘Communications’ menu within the ‘Settings’ menu.

Graphical user interface (GUI)

There is no screen lock. There is password protection for any configuration and settings changes.

The title and status bars are fixed. They remain in their locations regardless of where the user navigates to in the GUI. The icons and buttons on the title and status bars are fixed; however, the Favorites icon that is represented by an orange star in the status bar allows the user to create 9 GUI shortcuts.

Currently there is only a single level of password protection for the instrument. If the instrument is locked, access is at a ‘read only’ level. If the instrument is unlocked, configuration and settings changes are possible.

Operations

There is a start-up protocol that the iQ Series analyzer runs through with each power cycle. Alarms will be thrown with any issue as a result of the start-up protocol.  Notification and troubleshooting of those alarm notifications is identical to any alarm notification generated under normal run time.

Dual Range mode for the iQ instruments is identical to the comparable iSeries analyzer. However as opposed to discrete range setting selections that exist in iSeries, the iQ user can enter any value within the acceptable range for that instrument.

Service

The measurement technology is fundamentally the same so many of the mechanical parts of the measurement benches are the same between iSeries and iQ. The iQ DMC modules contain electronic/PCBA control which is different than iSeries. The components that are interchangeable/backwards compatible between iSeries and iQ on any given measurement bench are identified by part number in the manual.

There is no alarm history table created by the instrument. Similar to iSeries, you can log alarm history by configuring your data logging parameters to capture individual alarm states.

There is no prioritization to the assignment of alarm or maintenance notifications by the instrument, however, the way that those events generate email notifications is different. Upon power up, the analyzer waits 2 hours to clear any alarms prior to sending any email notifications. Post start-up sequence, an alarm needs to be active for 5 continuous minutes at which time an email notification will be generated and sent. The instrument will reflect an alarm condition on the status bar at any point that the instrument meets those alarm conditions, but an email will not be generated until any single alarm condition has existed for 5 continuous minutes. Maintenance notifications generated by either predictive diagnostics or the embedded preventive maintenance schedule behave in the same manner, except that the alert must be active for 24 hours prior to an email notification being sent.

The instrument configuration settings can be downloaded from the analyzer to USB.

There are a couple ways to uniquely identify each instrument. The ‘instrument ID’ or Modbus device ID is a user editable, numeric string. The instrument ‘host name’ is a user editable alpha-numeric string for mobile search functionality. The ‘host name’ can be used to access the instrument over TCP/IP but data download file names and reports will only reference the instrument serial number.

The embedded preventive maintenance schedule provides a warning when an item gets within 2 months of the replacement date. At that time, the line in the schedule will turn yellow and throws a ‘gear icon’ notification to the status bar. The line will change from yellow to red once the item gets within 1 month of the replacement date. The ‘gear’ icon will remain in place unless some activity is done to clear it.

The serialized DMC’s are unique to your analyzer and its configuration. To understand which DMC’s are serialized within your instrument, navigate to the ‘Health Check’ menu via the ‘Settings’ button on the home screen or the health check button on the status bar. From the ‘Health Check’ menu, click on ‘Status and Alarms’. The analyzer’s serialized DMC’s can be found by clicking on the ‘Serial Numbers’ button.


FAQs for particulate monitors

There are a number of features that allow the Models 5014iQ and 5030iQ to properly handle high sample loading. In the absence of wood smoke, the system will monitor the collected mass and the sample flow. If the collected mass exceeds a predetermined value, or if the sample flow rate decreases by more than 5%, the system will automatically advance the tape to a clean filter spot before the next scheduled tape advance, which is normally 8-hours. In the case of wood smoke, you may have high loading for wood smoke, but the collected mass may not be high enough to cause the tape to advance prior to the scheduled time. Because the instruments are using beta attenuation to monitor the mass, the measurements are not affected by the wood smoke composition and will accurately report the measured concentration.

 

One of the concerns that we are aware of with the design of beta monitors related to wood smoke, is that after a tape advance, the tape spot with collected wood smoke may stick to the O-rings in the measurement head of the instrument. The 5014iQ and 5030iQ have an option to increase the distance of the tape advance to ensure that the previously collected spot is moved away from O-rings in the measurement head. This setting is activated in the menu on the instrument. This is a manual setting that can be activated during periods when high wood smoke is present and deactivated after the wood smoke event passes. When activating this setting, the tape will be advanced twice as far as with the regular setting, resulting in a shorter interval requiring the tape replacement in the instrument.

Yes, white particulate can be measured. The color of the sample does not affect measurements by the beta detector. However, if the material is metallic with a high reflectivity, there may be a bias in the nephelometer measurement, but because of our design, we always correct the nephelometer readings so that the SHARP will match the beta.

Regulatory agencies have approved many technologies for monitoring ambient particulates. For example, Mass, Gravimetric, Beta, and Light Scattering/Optics are all approved technologies. Environmental conditions and your application needs play strong roles in identifying and selecting a suitable technology.

 

Under specific conditions such as wood smoke or high particulate loading, optics alone could report artificially high readings or measurement bias resulting in data inaccuracy, and hence such an instrument is not reliable choice. In such situations, Beta attenuation and Gravimetric technologies are better choices for accurate measurements, but these are limited by how fast data can be collected. Our 5030iQ monitor applies beta-correction to the optical readings to correct for any measurement biases and provides continuous data that is fast, reliable, and accurate.

Our 5014iQ monitor offers continuous sampling for faster data collection compared to the stepwise sampling offered on competitive beta monitors. Also, the 5014iQ monitor uses a longer 40m tape that requires tape replacements approximately once every year; competing products use much smaller tape, requiring tape replacements every 60 days.

 

Compared to light scattering-based technology monitors available in the market, the Thermo Scientific 5030iQ SHARP model stands out because it couples light scattering with beta technology to provide accurate data in real time. The beta attenuation confirms that any biases from light scattering caused by varying environmental conditions is corrected, thus delivering more accurate data for critical decision making. Depending on the environmental conditions and calibration shifts, monitors that rely solely on light scattering alone might provide data that is biased and therefore not accurate.

We, as the manufacturer of this product, have US regulatory approval and Nuclear Regulatory Commission (NRC) approval for our facility. Our monitors use a carbon-14 source with <100 microcurie. In the US it is exempt from hazardous material under Code UN2911, and no license is required. With such low C-14 levels, the NRC regards this as disposable in the trash.  Similarly, there is no special disposal requirement for the tape after its use and can be simply disposed in the trash. For other countries, please verify the requirements of the local regulatory agencies.

No, we have not. The half-life on C-14 is over 5000 years. It’s such a long time that it does not matter. Also, there is annual calibration of beta source to ensure proper function.

Negative measurement questions must be compared to current ambient conditions and other on-board diagnostics by reviewing instrument data. Also, understanding the reasons behind the negative readings is important for users to correctly interpret the data and understand their ambient environmental conditions.

 

Particulate matter (PM) can be heterogeneous, consisting of one or more elements including heavy metals; inorganic compounds such as salts; and semi-volatile components like organic carbon or secondary aerosols such as nitrates, sulfates, and water. Particles can exist in solid or liquid form or a mixture of both. PM is often hygroscopic, demonstrating an affinity for water at ambient RH of 75–80% or higher, and stubbornly retaining that bound water until experiencing a RH of less than 30–35%. In general, fine particles (PM-2.5) are more volatile than coarse particles. It is this complex characteristic that can lead to profound difficulty in consistent quantification of PM air pollution. The challenge is to provide a measure of PM under well-defined thermodynamic conditions (temperature, pressure, filter face velocity, and RH%). One must consider filter dynamics when discussing such situations.

Take the example of a complex mixture of particles collecting on our filter media. When the particulates collect on the filter, their mass may be influenced by interaction with airborne gases (acids, water vapor) or other particles in the sample air stream, or possibly by the filter media itself. The thermodynamic conditions of the sample air stream and the area around the sample filter influence the degree to which these ongoing reactions may occur. All these processes collectively comprise what we define as filter dynamics, and they may result in a positive or negative sampling artifact component of the PM mass concentration. The higher the time resolution of the PM measurement system, the more easily the PM mass concentration change resulting from filter dynamics can be observed. 

 

Regulatory methods employed for the determination of PM generate data that are defined to be an “indicator” of airborne PM. Regulatory standards are then based upon this indicator measurement. Note that the PM indicator measurement is to some degree determined by the definition, and it is not based purely upon scientific considerations. Almost all regulatory methods are “filter based” methods, centered around the measurement of PM collected on a sample filter.

 

The dynamics explained above describe how airborne particles can change because of their interaction with immediate surroundings, including the filter. Over a long time period, the net result of collecting these particles and measuring them is in a mass gain. This is true even though there may have been shorter periods when particles were losing mass due to negative artifacts. Only the faster-responding continuous methods of PM measurements are capable of seeing the short-term positive and/or negative mass changes that combine to make up the longer-term 24-hour measurement. A couple of examples help to highlight these points.

 

Example 1

 

A plume from a source such as a burn barrel, a wood-burning appliance or even a diesel vehicle engulfs a monitoring site. Should this happen, the short-term mass concentration will rise dramatically, followed by a sharp decrease after the plume ceases. The sharp decrease may be associated with a period (1 to 2 hours or more) of continuing net loss on the sample filter while the collected particulate matter continues to equilibrate to the thermodynamic conditions at the sample filter.

 

Example 2

 

Small water droplets from fog or mist are collected on the sample filter but evaporate over time. If the evaporative mass is greater than the collected mass, then net negative mass concentration is observed.

Yes, model 5014iQ would be a good choice for coastal areas with high humidity. The system will adjust the inlet heater to minimize the impact of changing and high humidity.

Yes, there is a setting to adjust parameters to accommodate seasonal variability.

The carbon vane pump ended with the legacy FH62C14 and Legacy 5030 SHARP monitors. The i-series and iQ-series now use a piston pump. The sample flow paths are same as the i-series.

The models 5014iQ and 5030iQ are mass measurement devices and are designed for monitoring TSP, PM10, PM2.5, and PM1. Considering the broader applicable definition of ultrafine particles as PM0.1, we do not have any data to confirm if these monitors can or cannot successfully monitor ultrafine particles, but if particles can be collected on the sample filter, the mass of the collected particles will be measured. If you have an inlet that will cut out particles greater than 0.1 um (the typical definition of ultrafine particles) and these are collected by the sample filter, the mass and concentration can be determined.

These monitors only do mass-based PM measurements and do not offer particle speciation. For a particle speciation type of analysis, it might be better to co-locate a Partisol sampler and use the sample collected on the filter for further analysis.

This would be difficult because the completed tape wraps upon itself. Also, to retrieve this information, you would need to cut the tape, which defeats the purpose of continuous monitoring. For this type of analysis, you might be better off to co-locate a Partisol sampler and use that sample filter for further elemental analysis without any compromise.

The beta detector is calibrated using zero and mass foils. There are different foils available at different mass levels and you can use the one that most closely aligns with the local concentration conditions.

These monitors function continuously and run at a 1-minute sampling rate. The internal instrument updates data every 10 seconds. The instrument’s algorithm performs some averaging and provides a readout once a minute.

Yes, these monitors are designed to be able to monitor multiple particulate sizes. Depending on your specific needs, these monitors can be used with sample inlets that have designated particulate cut-offs for TSP, PM10, PM2.5, and PM1.

Purchasing a new 5030iQ is always an option. However, if you no longer have need for your 5014iQ monitor and are seeking a 5030iQ monitor, you can easily upgrade to a 5030iQ monitor by using our 5014iQ upgrade kit option (Part number 109458-00). This upgrade kit can be used by our customers onsite. Customers are not required to ship the 5014iQ unit back to the factory for this product upgrade. With this, our customers get the benefit of cost savings and minimal to no downtime.

Yes, iQ series is designed to facilitate convenient replacement. It is our strong recommendation that our customers take advantage of this option and replace their legacy models with iQ series models when desired. The x-y position on the inlet is compatible with original i series monitor facilitating drop-in installation.

Service and product availability may vary by country and are subjected to varying regulatory requirements. Please contact your local sales representative for availability